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Latest research progress for LBE coolant reactor of China initiative accelerator driven system project

《能源前沿（英文）》 2021年第15卷第4期页码 810-831 doi: 10.1007/s11708-021-0760-1

摘要： China’s accelerator driven subcritical system (ADS) development has made significant progress during the past decade. With the successful construction and operation of the international prototype of ADS superconducting proton linac, the lead-based critical/subcritical zero-power facility VENUS-II and the comprehensive thermal-hydraulic and material test facilities for LBE (lead bismuth eutectic) coolant, China is playing a pivotal role in advanced steady-state operations toward the next step, the ADS project. The China initiative Accelerator Driven System (CiADS) is the next facility for China’s ADS program, aimed to bridge the gaps between the ADS experiment and the LBE cooled subcritical reactor. The total power of the CiADS will reach 10 MW. The CiADS engineering design was approved by Chinese government in 2018. Since then, the CiADS project has been fully transferred to the construction application stage. The subcritical reactor is an important part of the whole CiADS project. Currently, a pool-type LBE cooled fast reactor is chosen as the subcritical reactor of the CiADS. Physical and thermal experiments and software development for LBE coolant were conducted simultaneously to support the design and construction of the CiADS LBE-cooled subcritical reactor. Therefore, it is necessary to introduce the efforts made in China in the LBE-cooled fast reactor to provide certain supporting data and reference solutions for further design and development for ADS. Thus, the roadmap of China’s ADS, the development process of the CiADS, the important design of the current CiADS subcritical reactor, and the efforts to build the LBE-cooled fast reactor are presented.

关键词： LBE (lead bismuth eutectic) coolant reactor China initiative Accelerator Driven System (CiADS) project research progress

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中国ADS 铅基反应堆设计与研发进展 Review

吴宜灿

《工程（英文）》 2016年第2卷第1期页码 124-131 doi: 10.1016/J.ENG.2016.01.023

摘要：

2011年，在中国科学院战略性先导专项“未来先进核裂变能——加速器驱动次临界嬗变系统”等项目的支持下，针对加速器驱动次临界系统和第四代铅冷快堆的技术发展目标和试验要求，完成了具有临界和加速器驱动次临界双模式运行能力的10 MW中国铅基研究堆CLEAR-I的概念设计，建成了KYLIN系列铅铋回路试验平台，并在此基础上开展了反应堆冷却剂技术、关键组件、结构材料与燃料、反应堆运行与控制技术等铅铋反应堆关键技术的研发。为验证及测试铅基堆关键组件和综合操作技术，正在开展铅合金冷却非核反应堆CLEAR-S、铅基零功率核反应堆CLEAR-0和铅基虚拟反应堆CLEAR-V的建设。

关键词：加速器驱动次临界系统中国铅基反应堆铅铋共晶技术研发进展

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An old issue and a new challenge for nuclear reactor safety

F. D’AURIA

《能源前沿（英文）》 2021年第15卷第4期页码 854-859 doi: 10.1007/s11708-021-0729-0

摘要： Nuclear reactor safety (NRS) and the branch accident analysis (AA) constitute proven technologies: these are based on, among the other things, long lasting research and operational experience in the area of water cooled nuclear reactors (WCNR). Large break loss of coolant accident (LBLOCA) has been, so far, the orienting scenario within AA and a basis for the design of reactors. An incomplete vision for those technologies during the last few years is as follows: Progress in fundamentals was stagnant, namely in those countries where the WCNR were designed. Weaknesses became evident, noticeably in relation to nuclear fuel under high burn-up. Best estimate plus uncertainty (BEPU) techniques were perfected and available for application. Electronic and informatics systems were in extensive use and their impact in case of accident becomes more and more un-checked (however, quite irrelevant in case of LBLOCA). The time delay between technological discoveries and applications was becoming longer. The present paper deals with the LBLOCA that is inserted into the above context. Key conclusion is that regulations need suitable modification, rather than lowering the importance and the role of LBLOCA. Moreover, strengths of emergency core cooling system (ECCS) and containment need a tight link.

关键词： large break loss of coolant accident (LBLOCA) nuclear reactor safety (NRS) licensing perspectives basis for design of water cooled nuclear reactors (WCNR)

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铅冷快堆：未来的机会？ Vies & Comments

Alessandro Alemberti

《工程（英文）》 2016年第2卷第1期页码 59-62 doi: 10.1016/J.ENG.2016.01.022

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Experimental study of critical flow of water at supercritical pressure

Yuzhou CHEN, Chunsheng YANG, Shuming ZHANG, Minfu ZHAO, Kaiwen DU, Xu CHENG

《能源前沿（英文）》 2009年第3卷第2期页码 175-180 doi: 10.1007/s11708-009-0029-6

摘要： Experimental studies of the critical flow of water were conducted under steady-state conditions with a nozzle 1.41 mm in diameter and 4.35 mm in length, covering the inlet pressure range of 22.1-26.8 MPa and inlet temperature range of 38-474°C. The parametric trend of the flow rate was investigated, and the experimental data were compared with the predictions of the homogeneous equilibrium model, the Bernoulli correlation, and the models used in the reactor safety analysis code RELAP5/MOD3.3. It is concluded that in the near or beyond pseudo-critical region, thermal-dynamic equilibrium is dominant, and at a lower temperature, choking does not occur. The onset of the choking condition is not predicted reasonably by the RELAP5 code.

关键词： critical flow supercritical water-cooled reactor(SCWR) reactor safety loss of coolant accident(LOCA)

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Deep eutectic solvent inclusions for high- composite dielectric elastomers

《化学科学与工程前沿（英文）》 2022年第16卷第6期页码 996-1002 doi: 10.1007/s11705-022-2138-2

摘要： Recent advances in novel electroactive devices have placed new requirements on material development. High-performance dielectric elastomers with good mechanical stretchability and high dielectric constant are under high demand. However, the current strategy for fabricating these materials suffers from high cost or low thermal stability, which greatly hinders large-scale industrial production. Herein, we have successfully developed a novel strategy for improving the dielectric constant of polymeric elastomers via deep eutectic solvent inclusion by taking advantage of the low cost, convenient and environmentally benign synthesis process and high ionic conductivity from deep eutectic solvents. The as-prepared composite elastomers showed good stretchability and a greatly enhanced dielectric constant with a negligible increase in dielectric dissipation. Moreover, we have proven the universality of our strategy by using different types of deep eutectic solvents. It is believed that low-cost, easy-synthesis and environmentally friendly deep eutectic solvents including composite elastomers are highly suitable for large-scale industrial production and can greatly broaden the application fields of dielectric elastomers.

关键词： composite materials deep eutectic solvent dielectric elastomer high dielectric constant

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Surface modification by ligand growth strategy for dense copper bismuth film as photocathode to enhance

《能源前沿（英文）》 doi: 10.1007/s11708-023-0893-5

摘要： Hydrogen production from photoelectrochemical (PEC) water splitting has been regarded as a promising way to utilize renewable and endless solar energy. However, semiconductor film grown on photoelectrode suffers from numerous challenges, leading to the poor PEC performance. Herein, a straightforward sol-gel method with the ligand-induced growth strategy was employed to obtain dense and homogeneous copper bismuthate photocathodes for PEC hydrogen evolution reaction. By various characterizations, it was found that the nucleation and surface growth of CuBi₂O₄ layer induced by 2-methoxyethanol ligand (2-CuBi₂O₄) demonstrated a decent crystallinity and coverage, as well as a large grain size and a low oxygen vacancy concentration, leading to the good ability of light absorption and carrier migration. Consequently, under simulated sunlight irradiation (AM1.5G, 100 mW/cm²), the 2-CuBi₂O₄ photocathode achieved an enhanced photocurrent density of −1.34 mA·cm⁻² at 0.4 V versus the reversible hydrogen electrode and a promising applied bias photon-to-current efficiency of 0.586%. This surface modification by ligand growth strategy will shed light on the future design of advanced photoelectrodes for PEC water splitting.

关键词： copper bismuthate photocathode ligand growth strategy dense film PEC

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Directional solidification of metal-gas eutectic and fabrication of regular porous metals

LIU Yuan, LI Yanxiang, WAN Jiang

《机械工程前沿（英文）》 2007年第2卷第2期页码 180-183 doi: 10.1007/s11465-007-0030-x

摘要： Directional solidification of metal-gas eutectic (Gasar) is a novel process for making regular porous metals. This process is based on a solid-gas eutectic reaction involving a gaseous medium and a metal or ceramic phase. The process easily controls the porosity, the pore size, the pore orientation, and the pore morphology when the melting and solidifying conditions are varied in a wide range. The latest progress and our research work are reviewed in this paper.

关键词： orientation solid-gas eutectic research solidifying porosity

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Spontaneous polarization enhanced bismuth ferrate photoelectrode: fabrication and boosted photoelectrochemical

《能源前沿（英文）》 2021年第15卷第3期页码 781-790 doi: 10.1007/s11708-021-0782-8

摘要： In this paper, the fabrication of a highly orientated Bi₂Fe₄O₉ (BFO) photoelectrode in the presence of two-dimensional (2D) graphene oxide (GO) was reported. It was found that the GO can be used as a template for controlling the growth of BFO, and the nanoplate composites of BFO/reduced graphene oxide (RGO) with a high orientation can be fabricated. The thickness of the nanoplates became thinner as the ratio of GO increased. As a result, the ferroelectric spontaneous polarization unit arranges itself in the space in a periodic manner, leading to the formation of a polarization field along a special direction. Therefore, the created built-in electric field of the nanoplate composites of BFO/RGO is improved upon the increase of the amount of RGO. As expected, carrier separation is enhanced by the built-in electric field, therefore substantially enhancing the photoelectrochemical (PEC) activity of water splitting compared to pure BFO under the irradiation of visible-light.

关键词： bismuth ferrate ferroelectric polarisation photoelectrochemical (PEC) water splitting graphene oxide (GO) high orientation

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Enzyme@bismuth-ellagic acid: a versatile platform for enzyme immobilization with enhanced acid-base stability

《化学科学与工程前沿（英文）》 2023年第17卷第6期页码 784-794 doi: 10.1007/s11705-022-2278-4

摘要： In situ encapsulation is an effective way to synthesize enzyme@metal–organic framework biocatalysts; however, it is limited by the conditions of metal–organic framework synthesis and its acid-base stability. Herein, a biocatalytic platform with improved acid-base stability was constructed via a one-pot method using bismuth-ellagic acid as the carrier. Bismuth-ellagic acid is a green phenol-based metal–organic framework whose organic precursor is extracted from natural plants. After encapsulation, the stability, especially the acid-base stability, of amyloglucosidases@bismuth-ellagic acid was enhanced, which remained stable over a wide pH range (2–12) and achieved multiple recycling. By selecting a suitable buffer, bismuth-ellagic acid can encapsulate different types of enzymes and enable interactions between the encapsulated enzymes and cofactors, as well as between multiple enzymes. The green precursor, simple and convenient preparation process provided a versatile strategy for enzymes encapsulation.

关键词： bismuth-ellagic acid in situ encapsulation enzyme@MOF biocomposites

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ISA-YMG粗铅冶炼新工艺

王吉坤,周廷熙,冯桂林

《中国工程科学》 2004年第6卷第4期页码 61-66

摘要：

评述了铅提取技术的历史及现代铅提取技术的特点；针对我国目前粗铅冶炼现状，结合对高铅渣冶炼的多年研究，提出一种高效、节能、清洁的ISA-YMG粗铅冶炼新工艺，并提供了YMG还原熔炼工业试验结果。

关键词：铅ISA氧化熔炼高铅渣铅YMG还原熔炼粗铅冶炼新工艺

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Crystal design of bismuth oxyiodide with highly exposed (110) facets on curved carbon nitride for the

《化学科学与工程前沿（英文）》 2022年第16卷第7期页码 1125-1138 doi: 10.1007/s11705-021-2116-0

摘要： Crystalline materials with specific facet atomic arrangements and crystal facet structures exhibit unique functions according to their facet effects, quantum size effects and physical and chemical properties. In this study, a novel high-exposure (110) facet of bismuth oxyiodide (BiOI) was prepared (denoted as BiOI-110), and designed as nanosheets rich in oxygen vacancies by crystal facet design and regulation. Graphitic carbon nitride was designed as curved carbon nitride with dibromopyrazine, denoted as DCN, which contributed to a significant structural distortion in plane symmetry and improved the separation of charge carriers. Novel heterostructured BiOI-110/DCN nanosheets with a high-exposure (110) facet and abundant oxygen vacancies were successfully designed to enhance the photocatalytic degradation of organic pollutants. It was demonstrated that complete and tight contact between BiOI-110 and DCN was achieved by changing the size and crystal facet of BiOI. Oxytetracycline (OTC) and methyl blue dyes were used as targets for pollutant degradation, and 85.6% and 96.5% photocatalytic degradation efficiencies, respectively, were observed in the optimal proportion of 7% BiOI-110/DCN. The experimental results and electron spin resonance analysis showed that •O₂^– and h⁺ played a major role in the process of pollutant degradation. Additionally, high-resolution liquid chromatography-mass spectrography was used to identify the reaction intermediates of OTC, and the possible degradation pathway of this pollutant was proposed. Finally, the excellent reusability of BiOI-110/DCN nanomaterials was confirmed, providing a new approach for the removal of antibiotics that are difficult to biodegrade. Overall, crystal facet design has been proven to have broad prospects in improving the water environment.

关键词： high-exposure (110) facet oxygen vacancy-rich BiOI-110/DCN heterojunction photocatalytic degradation visible-light-response

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Modeling limit force capacities of high force to volume lead extrusion dampers

《结构与土木工程前沿（英文）》 2021年第15卷第3期页码 609-622 doi: 10.1007/s11709-021-0724-x

摘要： Lead extrusion dampers are supplemental energy-dissipation devices that are used to mitigate seismic structural damage. Small volumetric sizes and high force capacities define high-force-to-volume (HF2V) devices, which can absorb significant response energy without sacrificial damage. However, the design of such devices for specific force capacities has proven difficult based on the complexities of their internal reaction mechanisms, leading to the adoption of empirical approaches. This study developed upper- and lower-bound force capacity estimates from analytical mechanics based on direct and indirect metal extrusion for guiding design. The derived equations are strictly functions of HF2V device geometric parameters, lead material properties, and extrusion mechanics. The upper-bound estimates from direct and indirect extrusion are denoted as (F_UB,1, F_UB,2) and (F_UB,3, F_UB,4), respectively, and the lower-bound estimates are denoted as (F_LB, F_LB,1) based on the combination of extrusion and friction forces. The proposed models were validated by comparing the predicted bounds to experimental force capacity data from 15 experimental HF2V device tests. The experimental device forces all lie above the lower-bound estimates (F_LB, F_LB,1) and below the upper-bound estimates (F_UB,1, F_UB,2, F_UB,4). Overall, the (F_LB, F_UB,2) pair provides wider bounds and the (F_LB,1, F_UB,4/F_UB,1) pair provides narrower bounds. The (F_LB,1, F_UB,1) pair has a mean lower-bound gap of 36%, meaning the lower bound was 74% of the actual device force on average. The mean upper-bound gap was 33%. The bulge area and cylinder diameter of HF2V devices are key parameters affecting device forces. These relatively tight bounds provide useful mechanics-based predictive design guides for ensuring that device forces are within the targeted design range after manufacturing.

关键词： extrusion lead dampers upper and lower bound analytical modelling limit force

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Removal of lead from aqueous solution by hydroxyapatite/manganese dioxide composite

Lijing DONG,Zhiliang ZHU,Yanling QIU,Jianfu ZHAO

《环境科学与工程前沿（英文）》 2016年第10卷第1期页码 28-36 doi: 10.1007/s11783-014-0722-5

摘要： A novel composite adsorbent, hydroxyapatite/manganese dioxide (HAp/MnO ), has been developed for the purpose of removing lead ions from aqueous solutions. The combination of HAp with MnO is meant to increase its adsorption capacity. Various factors that may affect the adsorption efficiency, including solution pH, coexistent substances such as humic acid and competing cations (Ca , Mg ), initial solute concentration, and the duration of the reaction, have been investigated. Using this composite adsorbent, solution pH and coexistent calcium or magnesium cations were found to have no significant influence on the removal of lead ions under the experimental conditions. The adsorption equilibrium was described well by the Langmuir isotherm model, and the calculated maximum adsorption capacity was 769 mg·g . The sorption processes obeyed the pseudo-second-order kinetics model. The experimental results indicate that HAp/MnO composite may be an effective adsorbent for the removal of lead ions from aqueous solutions.

关键词： lead composite materials manganese dioxide hydroxyapatite adsorption

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Liquid metal as energy transportation medium or coolant under harsh environment with temperature below

Yunxia GAO, Lei WANG, Haiyan LI, Jing LIU

《能源前沿（英文）》 2014年第8卷第1期页码 49-61 doi: 10.1007/s11708-013-0285-3

摘要： The current highly integrated electronics and energy systems are raising a growing demand for more sophisticated thermal management in harsh environments such as in space or some other cryogenic environment. Recently, it was found that room temperature liquid metals (RTLM) such as gallium or its alloys could significantly reduce the electronics temperature compared with the conventional coolant, like water, oil or more organic fluid. However, most of the works were focused on RTLM which may subject to freeze under low temperature. So far, a systematic interpretation on the preparation and thermal properties of liquid metals under low temperature (here defined as lower than 0°C) has not yet been available and related applications in cryogenic field have been scarce. In this paper, to promote the research along this important direction and to overcome the deficiency of RTLM, a comprehensive evaluation was proposed on the concept of liquid metal with a low melting point below zero centigrade, such as mercury, alkali metal and more additional alloy candidates. With many unique virtues, such liquid metal coolants are expected to open a new technical frontier for heat transfer enhancement, especially in low temperature engineering. Some innovative ways for making low melting temperature liquid metal were outlined to provide a clear theoretical guideline and perform further experiments to discover new materials. Further, a few promising applied situations where low melting temperature liquid metals could play irreplaceable roles were detailed. Finally, some main factors for optimization of low temperature coolant were summarized. Overall, with their evident merits to meet various critical requirements in modern advanced energy and power industries, liquid metals with a low melting temperature below zero centigrade are expected to be the next-generation high-performance heat transfer medium in thermal managements, especially in harsh environment in space.

关键词： liquid metal cryogenics low melting point thermal management aircraft liquid cooling space exploration